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Calibration
Procedure for TDS Testr 1 and TDS Testr 2 with ATC
Even though the TDS Testr 1 and
TDS Testr 2 is factory calibrated, it is still necessary
to check the calibration against an appropriate standard
solution and recalibrate as needed. This is because
physical handling, temperature changes and the time
elapsed since the factory calibration makes it impossible
to guarantee the calibration still holds.
The TDS Testr 1 and TDS Testr
2 are like all other dissolved solids testers in that
they use the detected conductivity of a solution to
give a direct reading in ppm (parts per million) or
ppt (parts per thousand) of total dissolved solids
(TDS). The relationship between conductivity and TDS
is greatly affected by the types of dissolved solids
or salts present in the solution. It is absolutely
necessary to use a calibration solution similar
in dissolved solids content to the solution to be
tested in order to get acceptable accuracy. Also,
it is strongly recommended that the calibration solution
be at the same temperature as the test solution to
minimize temperature effect errors.
FACTORY CALIBRATION
Since there are many different types
of dissolved solids solutions that can be tested,
and since each type has its own "conductivity
to ppm of TDS" correlation, TDS Testr 1 and TDS
Testr 2 have been factory calibrated to selected TDS
formulations known as 442 formulations. The 442 formulation
closely approximates naturally occurring water from
lakes, wells and rivers. This factory calibration
is not appropriate for all possible applications and
it also is not possible to guarantee the calibration
will hold after the tester ships to the user. All
that can be guaranteed is that the TDS Testr 1 and
TDS Testr 2 can be calibrated to most of the more
commonly used TDS calibration standards, which are
within the measurement range of these models.
Therefore, it is necessary to re-calibrate
the TDS Testr 1 and TDS Testr 2 with an appropriate
calibration solution before using it in test solutions.
Options for obtaining an appropriate TDS standard
calibration solution are discussed at the end of these
instructions.
NOTE: Before the first use of the
TDS Testr series, it is necessary to soak the electrodes
in alcohol for three (3) minutes to remove oily residues.
Do not immerse the TDS Testr
into any liquid above the brown colored band.
INSTRUCTIONS
- The TDS Testr 1 and TDS Testr
2 are automatically temperature compensating (ATC),
however, it is strongly recommended that the TDS
standard calibration solution be at the same temperature
as the solution to be tested so as to minimize errors
from the temperature effect.
- Pour enough TDS standard
calibration solution into a clean and dry vessel
so that there is at least one inch of liquid.
- Remove the protective end
cap from the TDS Testr, exposing the stainless steel
electrodes.
- Turn the TDS Testr on with
the ON-OFF switch located on the front of the tester.
- Dip the TDS Testr electrodes
one-inch into the TDS standard calibration solution.
Make sure not to trap any air at the electrodes
or this causes errors in the readings. Tap the
tester gently on the bottom of the vessel to loosen
trapped bubbles.
Caution: Do not immerse the TDS Testr into any
liquid above the brown colored band.
- Allow the TDS Testr
electrodes to remain in the TDS standard calibration
solution until the reading stabilizes.
- Adjust the calibration
trimmer on the back of the TDS Testr so that the
digital display reading indicates the same value
as the TDS standard calibration solution value.
- Rinse the TDS Testr
electrodes with a portion of the liquid to be tested,
taking care not to use this rinse portion as a test
sample. This technique minimizes any carry over
contamination from the calibration solution and
eliminates the need to dry the TDS Testr electrodes.
If this is not practical, rinse the electrodes with
distilled water and air dry or blot dry using a
clean wipe.
- The TDS Testr is now
calibrated and ready to measure the TDS of your
test solution.
- Repeat this procedure
periodically to insure calibration.
NOTE: Increases in temperature of the sample
solution increases conductivity readings. The opposite
effect is true for decreases in temperature. The ATC
feature reduces this type of error so it is not as
significant. The TDS Testr will compensate for the
difference in temperature between your calibration
solution and the test solution with a coefficient
of 2% per °C (1.11% per °F) and will adjust
the displayed readings up or down accordingly.
SELECTING TOTAL DISSOLVED SOLIDS STANDARD CALIBRATION
SOLUTIONS
A total dissolved solids (TDS) standard calibration
solution should contain the same types of dissolved
solids known to be in the test solution. Failure to
do so will result in significant discrepancies between
the ppm or ppt reading and the actual ppm or ppt of
TDS in the test solution.
The easiest way to obtain total dissolved solids
standard calibration solution is to use a ready-made
standard solution that has the same types of dissolved
solids as the solution to be tested. These ready-made
solutions offer convenience and accuracy. They are
commonly formulated with either KCI, NaCI, CaCO3 or
a 442 natural water formulation (40% sodium sulfate,
40% sodium bicarbonate and 20% sodium chloride) to
meet the majority of applications. Choose a ready-made
calibration solution according to the following guidelines:
Choose a TDS standard calibration solution that contains
the same types of dissolved solids to be tested. Use
a TDS standard calibration solution that has a ppm
or ppt value as close as possible to the value of
the solution to be tested. If this is not reasonable
because of the variations in the test solution, it
is best to calibrate the TDS indicator with a TDS
standard that has a ppm or ppt value in the upper
one-third of the TDS indicator's measurement range.
The following is a list of ppm TDS standard calibration
solutions available for OAKTON Instruments, with their
contents and applications described. Standardization
values of the calibration solutions are based on conditions
of 25°C.
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Application
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Part number
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Use With
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Adjust display to
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TDS of KCI solutions, brines,
general purpose TDS measurements
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WD-00653-20
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TDS Testr 1
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1380 ppm
1pt.
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TDS of lake,
stream, well waters, boiler and cooling tower
feed waters, general water treatment
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WD-00653-47
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TDS Testr 1
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330 ppm (442*)
220 ppm
(NaCI for brines)
1 pt.
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TDS of lake,
stream, well waters, boilers and cooling tower
feed waters, general water treatment, rinse
water and brines
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WD-00653-27
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TDS Testr 1
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1500 ppm (442*)
1040 ppm (NaCI)
1 pt.
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TDS of lake,
stream, well waters, boiler and cooling tower
waters, general water treatment, waste water
and brines
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WD-00653-89
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TDS Testr 2
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7.61 ppt (442*)
7.23 ppt (NaCI)
1 pt.
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*442 is a formulation of 40% sodium
sulfate, 40% bicarbonate and 20% sodium chloride that
is used as a TDS Standard for testing natural waters
(i.e. lakes and streams) and boiler and cooling tower
waters
It is possible that the above list
will not contain a calibration solution appropriate
for some applications. One solution to this problem
is to have "tailor-made" ppm TDS standard
calibration solutions. This is done by formulating
a mixture of salts in relative proportions that simulate
the solution to be tested, and then dissolving this
mixture into distilled water. This should be performed
according to the formula:
1 mg salt mixture / liter of distilled water
= 1 ppm TDS or, in other words
X ppm TDS = X mg of salts + one liter of distilled
water
Remember that "X" mg of salts is the number
of milligrams of a mixture of salts that's proportions
simulate your test solution, NOT "X" milligrams
of each salt in the mixture.
An appropriate value for "X" is determined
by the following rule:
Try to choose a ppm or ppt for a calibration solution
as close as possible to the expected ppm or ppt values
of the test solutions. If the test solution's TDS
value is expected to vary a great deal, it is best
to choose a ppm or ppt value for the calibration solution
that is in the upper one-third of the TDS indicators
measurement range.
"Tailor-made" solutions such as these are
common and can be made by the operator of the meter
or they can be purchased at a local testing laboratory.
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